Experimental Investigation of Thermal Properties of Binary Metal Alloys
| Autoři | |
|---|---|
| Rok publikování | 2019 |
| Druh | Další prezentace na konferencích |
| Fakulta / Pracoviště MU | |
| Citace | |
| Popis | In our work we developed synthetic strategies for preparation of alloy nanoparticles of Bi, Ni and Sn in which we used a reduction route. NaBH4 and BH3.H2NtBu were used to reduce particular metal salts to obtain nanoparticles of zero-valent metal alloys. Polyvinylpyrrolidone or 1,10-phenanthroline were used as surfactants to stabilize their surface. Prepared NPs, their phases and phase transformations were studied by Powder X-Ray Diffraction (PXRD), Transmission and Scanning Electron Microscopy (TEM, SEM/EDS) (Fig. 2) and Differential Scanning Calorimetry (DSC). The results were compared with both bulk and nano phase diagrams and were in good agreement with theoretical predictions. |
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