NEHYDROLYTICKÉ METODY PŘÍPRAVY FOSFOSILIKÁTOVÝCH A TITANOSILIKÁTOVÝCH MATERIÁLŮ

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Title in English	Nonhydrolytic methods for the synthesis of phosphosilicate and titanosilicate materials
Authors	STÝSKALÍK Aleš ŠKODA David PINKAS Jiří MORAVEC Zdeněk
Year of publication	2009
Type	Article in Proceedings
Conference	ChemZi
MU Faculty or unit	Faculty of Science
Citation
Field	Inorganic chemistry
Keywords	phosphosilicates; titanosilicates; sol-gel; nonhydrolytic reactions
Description	We developed new nonhydrolytic methods for the synthesis of phosphosilicate and titanosilicate materials based on ester elimination from silicon acetate and tris(trimethylsilyl)ester of phosphoric acid or titanium isopropoxide. Obtained xerogels were analyzed by IR spectroscopy, thermal analysis TG-DSC, XRD powder diffraction, ICP-OES, 29Si and 31P CPMAS NMR spectroscopies.
Related projects:	Physical and chemical properties of advanced materials and structures