Influence of physical properties and chemical composition of sample on formation of aerosol particles generated by nanosecond laser ablation at 213 nm

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Authors

HOLÁ Markéta KONEČNÁ Veronika MIKUŠKA Pavel KAISER Jozef KANICKÝ Viktor

Year of publication 2010
Type Article in Periodical
Magazine / Source Spectrochimica Acta Part B
MU Faculty or unit

Faculty of Science

Citation
Field Analytic chemistry
Keywords Laser ablation; Inductively coupled plasma; Mass spectrometry; Aerosol; Tungsten carbide; steel; glass
Description The influence of sample properties and composition on the size and concentration of aerosol particles generated by nanosecond Nd:YAG laser ablation at 213 nm was investigated for three sets of different materials, each containing five specimens with a similar matrix (Co-cemented carbides with a variable content of W and Co, steel samples with minor differences in elemental content and silica glasses with various colors). The concentration of ablated particles (particle number concentration, PNC) was measured in two size ranges (10-250 nm and 0.25-17 mu m) using an optical aerosol spectrometer. The shapes and volumes of the ablation craters were obtained by Scanning Electron Microscopy (SEM) and by an optical profilometer, respectively. Additionally, the structure of the laser-generated particles was studied after their collection on a filter using SEM.
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